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Certain cobalt(II) complexes such as the cobaloxime XXVIIa and the corresponding boron uoride XXVIIb (L is a ligand) terminate propagating chains by a transfer reaction called

catalytic chain transfer (CCT) [Chiefari and Rizzardo, 2002; Gridnev, 2000; Gridnev and Ittel, 2001; Heuts et al., 2002; Roberts et al., 2003]. The overall result is the transfer of an H atom from a propagating chain to monomer, but the process occurs by a two-step mechanism (Eqs. 3-132, 3-133) in which Co(II) acts as a catalyst. In the rst step, an H atom is

CH3 CH2 C COOR CH3 CH2 C COOR + Co(III) H CH3 C COOR + Co(II) CH2 CH2 C COOR CH3 + Co(II)

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The system at first developed slowly In 1864 a new law provided convenient provisions for the conversion of state banks into national associations In 1865 a law taxed the issue of state banks at 10% and thus forced state bank notes into retirement After the war was over the new National Banking System dominated the currency and the market for government bonds However, after 1882 the application of a chronic Treasury surplus to the reduction of the national debt reduced the volume of bonds that could be held by the banks to secure circulation, while at the same time individuals, trustees, and corporations were seeking to buy government bonds for investment The bonds advanced to such high premiums that it became unprofitable for the banks to retain them even with the circulation privilege; as a consequence note circulation declined.

Although we re usually interested in ICs, here you ll be looking mainly to connect a one-shot pushbutton to a couple of lone components further down the board (see bending diagram, Figure 18-2). It s interesting to note that although the battery compartment is located on the back half of the case, the battery contacts are located on the board right there in front of you. Keep this in mind as you run your wires. Just imagine the batteries lying between the battery contacts (the stiff wires rising from the board) and keep all wires from crossing this area.

3-133

+ Co(III)

3-132

The redemption yields of some bonds were at times negative, even when short-term interest rates were very high Congress was urged to accept other forms of bank assets as security for the currency or to fund high-rate government bonds into new issues at low nominal rates running for long periods of time and not subject to redemption..

transferred from the propagating chain to Co(II) to form Co(III) hydride, which subsequently transfers the H atom to monomer to reinitiate polymerization. Note that catalytic chain transfer differs from chain transfer to monomer (Sec. 3-6b-2). Chain transfer to monomer results

FIGURE 18-2: Bending diagram for the Casio SA-2 Aleatron. Capacitor C2 s upper lead is the same as the IC pin that one of the body-contacts connects to (C2 is two capacitors to the right of the target IC pin). If C2 s lead that is closest to the chromed battery spring is accessible, you can solder the body-contact wire there instead.

in a polymer molecule with a saturated end group by transfer of an H or other atom from monomer to propagating chain Catalytic chain transfer involves transfer of an H atom in the opposite direction (from propagating chain to monomer) and results in a polymer molecule with an unsaturated end group The reaction is catalytic because the transfer agent is regenerated in the second step Various cobaloximes and cobaloxime boron uorides have been examined R can be alkyl or aryl Various ligands have been used, including Cl, Pf3, methanol, and pyridine, and combinations thereof Cobalt prophyrins have also been found to be effective CCT agents Active CCT agents based on metals other than cobalt have not yet been found Catalytic chaintransfer agents are much more active in chain transfer than the most active conventional chain-transfer agents discussed previously.

of the following two issues, each of which was convertible into such higher-rate bonds as might be issued during the war: 1917 $2.0 billion 3.8 billion First Liberty Loan 31 2s, redeemable in 1932, due 1947, tax-exempt; sold at 100 = 3.50%. Second Liberty Loan 4s, redeemable in 1927, due 1942, partially tax-exempt (P.T.E.: partially tax-exempt government bonds were exempt from the normal income tax but subject to the surtax); sold at 100 = 4%.

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